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the gluten.

From here the starch-phate of barium may be used, or any milk is conveyed to the inclined other barium salt forming an insoluble starch tables G, and is then carried combination. into a channel at the head of the series of tables where it is comminuted by a revolving knife, water being admitted at the same time. The paste is conveyed to the mixing reservoir K provided with a stirring apparatus, and finally into the settling box L, where it is washed. To produce glucose the starch is brought into the open converter L, drawn off into the holder M, and here neutralized. The fluid is then conducted through the settling box M' and the bag-filter M' into the reservoir M', and bleached. From M' the fluid passes through the bag-filter N' to N' and O, is filtered through animal charcoal, and then pumped into the vacuum pan Q, where it is concentrated. After passing through the filtering press R, it is ready to be drawn into barrels.

For preparing hard grape sugar (dextrose), the solution of sugar is conveyed from the closed converter L into the reservoir T, then to T' where it is neutralized and bleached, and finally into the settling box M. From here it is passed through the bag-filter M2 into the reservoir M3, filtered, then pumped into M', where it is bleached and filtered through N into N'. From the latter it is conveyed to O, and is either filtered through the carbon filter P or brought directly into the vacuum pan Q. The concentrated fluid is filtered through filter-presses into U, and passes from here into the cooling apparatus. SV and V' are the steam apparatus and furnace for revivifying the animal charcoal. In the cooling apparatus S the hot cream-like sugar is kept in constant motion by a screw, and cooled off by serpentine pipes. Solidification is accelerated by throwing in finished sugar.

To Remove Gypsum from Solutions of Glucose produced with the aid of Sulphuric Acid. The solution of glucose formed by boiling the starch with dilute sulphuric acid is, after being neutralized with chalk, filtered, compounded with oxalate of barium and boiled down. The solution, after filtering, is entirely free from gypsum. In place of oxalate of barium, phos

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Preparation of Pure Levulose. Prepare a 10 per cent. solution of cane sugar, add for every 100 parts of sugar 2 parts of hydrochloric acid, and heat to 140° F. At this temperature the fluid remains entirely colorless. The conversion into grape and fruit sugars takes place very slowly and regularly, 1 pounds of sugar requiring about 17 hours. After complete conversion a 12 per cent. solution of inverted sugar is obtained. Allow the fluid to cool slowly to about 23° F. Then add to every 10 parts of sugar 6 parts of slaked lime pulverized and passed through a hair sieve, mix and stir thoroughly. The fluid congeals to a paste, the temperature rising about 2 degrees. Then press out the paste in order to separate the liquid lime-compound of grape sugar from the solid lime-compound of fruit sugar. place the latter in water and press it out again, repeating the operation as long as the wash-water turns to the right. The remaining mixture of lime-compound of levulose and excess of lime is suspended in water and saturated with oxalic acid until the lime-compound is accurately neutralized. The scarcely yellowish colored fluid is then filtered off from the oxalate of lime into a large beaker glass and placed in a cold mixture of snow and hydrochloric acid. Stir thoroughly until about of the water is frozen. Then throw the whole upon a linen filter, and, as soon as the greater part of the fluid is drained off, press out the residue. Replace the combined filtrates in the cold mixture and repeat the whole process until a very concentrated solution of levulose is obtained, and then dry the levulose syrup in a vacuum. Levulose thus obtained is pure and white.

A New Source for Supplying Mannite is, according to W. Thörner, the Agaricus integer, a common and easily recognized fungus. Boil out the comminuted fungus with fresh quantities of alcohol until the extracts, on cooling, separate no more crystals. The crystalline mass, consisting of separated mannite, is redissolved in alcohol and

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Fig. 40.-Jepp's Apparatus for Fabrication of Starch, Glucose, and Grape Sugar.

Purification of Sugar Beet Juice by means of Silica Hydrate. Heat the juice nearly to the boiling point and compound it with to 2 parts of silica hydrate of 10° B. to every 100 parts of juice, the quantity depending on the organic substances and organic alkaline combinations in the juice. In about 5 minutes add to the mixture 0.004 per cent. of lime in the form of milk of lime (or air-slaked) and then let it come to a boil. Remove the resulting precipitate by pressing and treat the filtrate like other juice, i. e., filter and boil down.

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boiled with animal charcoal. From perature will, if continued for a longer the filtered fluid the mannite crystal-period, slightly change the color of lizes in snow-white needles. One hun- white wool, cotton, silk, and dred parts of Agaricus integer yield bleached linen, but will not otherwise from 19 to 20 parts of mannite. injure them. A heat of 293° F., continued for about 3 hours, slightly singes white wool, and less so unbleached and white cotton, white silk, and linen, both unbleached and white, but does not materially injure their appearance. The same heat continued for about 5 hours singes and injures the appearance of white wool and cotton, unbleached linen, white silk, and some colored fabrics of wool, or mixed wool and cotton, or mixed wool and silk. It is noteworthy that the singeing of any fabric depends not alone upon the heat used, but also on the time during which it is exposed. In these experiments the heat was obtained by burning gas with smokeless flames, and conducting the products of combustion, mixed with the heated air, by means of a short horizontal flue into a cubical chamber through an aperture in its floor, and out of it by a smaller opening in its roof. Fixed thermometers showed the temperature of the entering and outgoing currents, which represent the maximum and minimum temperatures of the chambers.

To Prepare Strontia Sugar from Treacle and Syrup. By using 3 molecules of strontia to 1 molecule of sugar strontium saccharate is precipitated at the boiling point under ordinary or higher pressure. The precipitate is separated from the fluid in a hot condition and washed with hot water. The strontium saccharate thus obtained is decomposed by water at a lower temperature into basic saccharate and free strontium hydrate. The strontium saccharate is used for separating beet juice and other sacchariferous juices.

TEXTILE FABRICS AND TISSUES.

Coating Textile Fabrics with Metallic Substances. Fine comminuted metallic powder is mixed with an adhesive substance, as caoutchouc, etc., and the mixture applied either by hand or machine to the textile fabric, which is then dried and glazed. After glazing a pattern may be either pressed or printed upon the fabric.

Effect of Heat on Textile Fabrics. Recent experiments have shown that white wool, cotton, and silk may be heated to 248° F. for 3 hours without apparent injury, except that wool will show a slight change in color, especially when new. The same may be said of dyed wools, printed cottons, and most dyed silks; but some white silks turn brown by this heat, and some pink silks are faded by it. The same tem

Feather-plush. A process has recently been patented in Germany whereby finely comminuted down is worked with textile materials into a fur-like fabric, in lengths of about 50 yards by 2 yards in width. The down may also be used in the manufacture of light bed-covers, wall-papers, etc., and for this feathers of little or no value and formerly considered useless can be utilized. The process is as follows: The feathers are comminuted by a machine representing a combination of a batting machine, fan and sieves. The resulting down is then carded in a carding engine together with 40 to 90 per cent. of other material and formed into a close fleece. By mechanical friction and the aid of steam the fleece is joined together in large pieces of a kind of felt, which is then converted into a cloth-like material by the fulling process. The resulting fabric is then thoroughly dried and steamed for some time at a very high temperature in a closed steam-box, resembling an appa

ratus for shrinking cloth. By this pro- | after the drawing has been removed, cess an intimate union is formed be- is washed. A very fusible metal, the tween the down and the other materials, Spence metal being the best adapted the fabric assuming at the same time a for the purpose, is then poured over the plush-like appearance, which can be chrome-gelatine surface. The casting very much varied in the finishing. can be directly used, or fac-similes are prepared with the help of this metalplate, either by the galvanoplastic or some other process.

Down-cloth. Seventy-nine to 85 parts of down are mixed with 20 to 30 parts of wool and 50 to 60 parts of oleic acid. The mixture is then passed through a batting machine, and then worked in succession in a breaking card, finishing card, and carding machine. The material is then spun and woven. The finished piece is freed from oil, fulled, raised, shorn, and dyed. The card-clothing of the rollers of the carding machine corresponds to the material to be worked. On the finishing card is arranged an endless cloth upon which rests another endless cloth, which receives the mixture from the porcupine, and, carrying it along, is wound with it around a roller. On the carding engine is also arranged an endless cloth upon which the fleece wound around the roller of the finishing card is unrolled and carried by it to the working rollers. There is a further contrivance on the carding engine by which one or more threads may be introduced into the roving in order to make the fabric more durable. The improvements in the gig consist in an arrangement of drums covered with carding between which the piece of cloth runs.

Improvements in the Treatment of Vegetable Fibres. The fibres after having been freed from foreign constituents are bleached in a bath of to 1 per cent. of ethyl chloride to 25 gallons of water. To give to them a silk-like gloss they are immersed for 3 hours in a bath of sodium carbonate or bicarbonate, then exposed to the fumes of burning sulphur, and finally thoroughly rinsed with water.

To give greater flexibility to the fibres, they are, after having been dried over hurdles, submitted to the action of glycerine vapors.

Improvement in the Preparation of Surfaces to be Printed on, Embossed,

etc.

A design or drawing on transparent paper is placed upon a layer of chrome-gelatine and exposed to the light. The surface of chrome-gelatine,

In place of the design a drawing prepared by weaving, knitting, printing, etc., can be used. Such drawing is then coated with a thick coat of coloring matter or plastic material. In case the relief formed is not deep enough, it is improved by scattering any powder or fibrous substance upon the surface while it is still in a plastic state. It is then filled up with Spence metal, and the resulting plate used for printing. This process is also available for printing with type and for embossing.

New Method of Compressing the Fibres of Cotton Tissues, and Giving the Colors more Lustre. This invention is based upon the fact that cotton threads treated with cold caustic-lye are compressed to. By this process apparently very fine tissues can be prepared from coarser, the colors appearing more intense and brilliant. The fabric gains in strength. A thread which would formerly break when loaded with 14 ounces will, after treatment, require a weight of 21 ounces.

New Yarn, called Pearl Yarn, consists of threads upon which at any desired intervals are fastened drops or pearls of a pasty substance, which, on congealing, assume the appearance of glass or crystals. The substance is prepared from wax, rosin, lacquer, gum, and enamel. The pearl yarn is prepared either by hand or a trough is used for the reception of the paste. Tubes are arranged in the trough, each of which is provided with an aperture below, from which a drop of the pearl substance exudes and is received by a thread held under the tube.

Oil-cloth. The customary process of stretching the tissue in a frame and coating it with a vegetable gluten makes the oil-cloth hard and brittle. It is claimed that animal gelatine, substituted for the vegetable gluten, remedies this defect. Boiling the pit of the

horns of ruminants makes the best gelatine for this purpose, the ordinary glue and gelatine not giving equally good results. To about 32 parts of melted gelatine add part of a saponifying material (borax being the best) and 16 parts of linseed-oil varnish, and allow the compound to congeal. Then bring it into a mill and mix it with 30 parts of mineral color soaked in water, such as kaolin, chalk, etc. Reduce the compound with naphtha, and bring it into the priming machine, where it may be applied to the tissue once or oftener. When the ground is sufficiently dry, the following composition is applied: 75 parts of kaolin are formed into a thick paste with water mixed in a mill with 33 parts of linseed-oil varnish and reduced with naphtha. Kaolin mixed with linseed-oil varnish has been pre viously used for the same purpose, but the kaolin having been mixed in a dry state with the varnish, the oil-cloth remained in consequence hard and brittle. Soaking the kaolin before mixing it with the varnish remedies this evil. The composition is also applied to the cloth by means of the priming machine, adding at the same time the ground color the oil-cloth is to have, and it finally receives the desired pattern in the ordinary way.

Apparatus and Process for Scouring and Removing the Oil from Fleece, Wool, and Silk, and Woollen Fabrics of every Description. The process is based upon the use of carbonic acid gas or carbonated water as a washing agent, with or without other ingredients generally used for washing, cleansing, and bleaching. The apparatus used consists of a revolving wash-barrel containing the

Fig. 41.

fabrics to be manipulated. The carbonic acid gas or carbonated water enters through the tube a (Fig. 41), and

steam from the opposite side through the tube b. Both steam and carbonic acid are converted into a fine spray by means of a perforated tube inside the barrel. c is the carbonic acid holder, d is a wagon for carrying away the fabrics, e the cover of the aperture through which the barrel is filled and emptied, f the safety-valve, g the escapepipe for the gases.

Process for Animalizing Vegetable Fibres with Nitro-glucose (Nitro-saccharose). Nitro-glucose or saccharose is prepared by treating sugar with nitric or sulphuric acid and washing and kneading. The product is dissolved in acetic acid or methyl-alcohol, and the vegetable fibres are saturated with the solution. The nitro-glucose may also be produced upon the tissue by immersing it in a solution of sugar and submitting it to the action of nitric acid vapors or drawing it through a solution of the acid. Fibres prepared in this manner act in dyeing like animal substances.

Patent Process to give to Colored Fabrics a Metallic Lustre. For 5 parts of black tissues use a bath consisting of: Water 500 parts, sulphate of copper

part, and tartaric acid part. The tissues are manipulated in this at a moderate heat for half an hour, then rinsed, placed in a decoction of 5 parts of logwood and some ebony shavings with the corresponding quantity of water, again rinsed and dried. They are then placed in a mixture of part of sulphate of copper, 14 parts of aqua ammonia, and 500 parts of water at a temperature of 167° to 190° F., for 12 to 15 minutes. They are then rinsed, and finally brought into solution of sodium hyposulphite of 25° B., again rinsed and dried.

Preparation of Fibres that can be Spun from Nettles, Hemp, Jute, etc. To facilitate the action of the chemicals used in the process the stems, which are generally very hard and woody, must be broken. This is best accomplished by passing the stems between fluted rollers and exposing them in a suitable vessel for a few hours to the action of steam, which separates the woody parts from the fibres, removes the vegetable gum mucus, etc., by loosening the substances enclosing the fibres. To make the action of the steam more effective,

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